N,N'-二甲基-1,4-丁二胺合成路线 （共 19 条）
反应条件
1: water 2: chloroform; thionyl chloride View Scheme
参考文献
Ishidate et al.
Chemical and Pharmaceutical Bulletin, 1958 , vol. 6, p. 164,168
反应条件
1: water 2: chloroform; thionyl chloride 3: hydrogen peroxide; diethyl ether / anschliessend mit Acetanhydrid View Scheme
参考文献
Ishidate et al.
Chemical and Pharmaceutical Bulletin, 1958 , vol. 6, p. 164,168
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 5 p. 1207 - 1208,1081
反应条件
1: hydrogenchloride / methanol / 0 - 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / |Reflux
View Scheme
参考文献
Jang, Sun Jeong; Choi, Heung Woo; Choi, Doo Li; Cho, Sehyeon; Rim, Hong-Kun; Choi, Hye-Eun; Kim, Ki-Sun; Huang, Minghua; Rhim, Hyewhon; Lee, Kyung-Tae; Lee, Jae Yeol
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 24 p. 6656 - 6662
参考文献
Higley, David P.
Patent: US2003/45674 A1, 2003 ;
反应条件
in ethanol
Michael addition;
参考文献
Ullah, Nisar; Haladu, Shamsuddeen A.; Mosa, Basem A.
Tetrahedron Letters, 2011 , vol. 52, # 2 p. 212 - 214
