2-氯-6-羟基-7-甲基嘌呤合成路线 （共 7 条）
参考文献
Boehringer and Soehne
Patent: DE96925 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 5, p. 846
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Fischer,E.
Chemische Berichte, 1897 , vol. 30, p. 2414
Chemische Berichte, 1898 , vol. 31, p. 545 Anm.
反应条件
1: phosphorus oxychloride / 140 °C 2: diluted NaOH-solution View Scheme
参考文献
Fischer,E.
Chemische Berichte, 1897 , vol. 30, p. 2414
Chemische Berichte, 1898 , vol. 31, p. 545 Anm.
反应条件
1: 51 percent / 20percent aq. KOH / H2O; methanol / 1 h / 30 °C / pH = 9 2: 45 percent / propan-1-ol / 2 h / 60 °C 3: 18percent aq. HCl / 1.5 h / Heating View Scheme
参考文献
Kowalska, Alicja; Maslankiewicz, Andrzej; Syrek, Barbara; Cieplinski, Piotr
Monatshefte fuer Chemie, 1985 , vol. 116, p. 341 - 352
反应条件
potassium hydroxide in methanol; water T=30°C; 1 h; pH = 9;
参考文献
Kowalska, Alicja; Maslankiewicz, Andrzej; Syrek, Barbara; Cieplinski, Piotr
Monatshefte fuer Chemie, 1985 , vol. 116, p. 341 - 352
反应条件
1: 51 percent / 20percent aq. KOH / H2O; methanol / 1 h / 30 °C / pH = 9
2: 60 percent / ethanol / 2 h / 60 °C
3: 1 h / 165 - 170 °C
View Scheme
参考文献
Kowalska, Alicja; Maslankiewicz, Andrzej; Syrek, Barbara; Cieplinski, Piotr
Monatshefte fuer Chemie, 1985 , vol. 116, p. 341 - 352
反应条件
1: 51 percent / 20percent aq. KOH / H2O; methanol / 1 h / 30 °C / pH = 9
2: 45 percent / propan-1-ol / 2 h / 60 °C
3: 1 h / 165 - 170 °C
View Scheme
参考文献
Kowalska, Alicja; Maslankiewicz, Andrzej; Syrek, Barbara; Cieplinski, Piotr
Monatshefte fuer Chemie, 1985 , vol. 116, p. 341 - 352
反应条件
NaSH*1.5H2O in N,N-dimethyl-formamide
2 h; Heating;
参考文献
Kowalska, Alicja
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 12 p. 2881 - 2890
