反应条件
1: trichlorophosphate / 4 h / |Inert atmosphere; |Reflux 2: sodium hydride / tetrahydrofuran / 3 h / |Inert atmosphere; |Reflux 3: ozone / dichloromethane; methanol / -78 - 20 °C / |Inert atmosphere 4: triethylamine; trifluoromethanesulfonic anhydride / dichloromethane / 15 h / 5 - 20 °C View Scheme
参考文献
Katamreddy, Subba R.; Carpenter, Andrew J.; Ammala, Carina E.; Boros, Eric E.; Brashear, Ron L.; Briscoe, Celia P.; Bullard, Sarah R.; Caldwell, Richard D.; Conlee, Christopher R.; Croom, Dallas K.; Hart, Shane M.; Heyer, Dennis O.; Johnson, Paul R.; Kashatus, Jennifer A.; Minick, Doug J.; Peckham, Gregory E.; Ross, Sean A.; Roller, Shane G.; Samano, Vicente A.; Sauls, Howard R.; Tadepalli, Sarva M.; Thompson, James B.; Xu, Yun; Way, James M.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 24 p. 10972 - 10994