(r)-1-三苯甲游基-2-氮丙啶羧酸甲酯合成路线 (共 7 条)
反应条件
methanesulfonyl chloride; triethylamine in tetrahydrofuran Heating; Yield given;
参考文献
Kato, Shiro; Harada, Hiroshi; Morie, Toshiya
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 21 p. 3219 - 3225
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in chloroform Heating; Yield given;
参考文献
Ki, Duk Park; Morieux, Pierre; Salome, Christophe; Cotten, Steven W.; Reamtong, Onrapak; Eyers, Claire; Gaskell, Simon J.; Stables, James P.; Liu, Rihe; Kohn, Harold
Journal of Medicinal Chemistry, 2009 , vol. 52, # 21 p. 6897 - 6911
反应条件
1: Et3N 2: Py 3: Et3N / tetrahydrofuran / Heating View Scheme
参考文献
Kato, Shiro; Harada, Hiroshi; Morie, Toshiya
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 21 p. 3219 - 3225
反应条件
1: pyridine / 22 h / 0 °C 2: Et3N / tetrahydrofuran / 22 h / Heating View Scheme
参考文献
Axelsson, B. Svante; O'Toole, Kevin J.; Spencer, Philip A.; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 7 p. 807 - 816
反应条件
chloroform Behandeln mit Tritylchlorid und Methansulfonylchlorid und Erwaermen des Reaktionsgemisches unter Zusatz von Methanol;
参考文献
Smrt et al.
Experientia, 1957 , vol. 13, p. 291
Collection of Czechoslovak Chemical Communications, 1957 , vol. 22, p. 262,270
反应条件
perchloric acid 30 h; Heating;
参考文献
Axelsson, B. Svante; O'Toole, Kevin J.; Spencer, Philip A.; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 7 p. 807 - 816
反应条件
trifluoroacetic acid in methanol; chloroform
T=0°C; 2.5 h;
参考文献
Church, Nicola J.; Young, Douglas W.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 9 p. 1475 - 1482