2-(2-甲氧基乙氧基)乙酸合成路线 (共 8 条)
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hydrogencarbonate; sodium carbonate T=20°C; 2.5 h; Electrochemical reaction;
参考文献
Kuroboshi, Manabu; Yoshida, Tomonori; Oshitani, Jun; Goto, Kuniaki; Tanaka, Hideo
Tetrahedron, 2009 , vol. 65, # 34 p. 7177 - 7185
参考文献
Journal of the American Chemical Society, , vol. 62, p. 1635,1637
Chemische Berichte, , vol. 63, p. 3119
US2010154 , ;
反应条件
hydrogenchloride; sodium acetate
参考文献
Journal of Chemical Research, Miniprint, , # 7 p. 1701 - 1720
反应条件
hydrogen bromide T=20 - 150°C; 8 h;
参考文献
Grablowitz, Hans; Lendlein, Andreas
Journal of Materials Chemistry, 2007 , vol. 17, # 38 p. 4050 - 4056
反应条件
hydrogen bromide in water T=0°C; pH=3; Reflux;
参考文献
Koissi, Niangoran; Shah, Niti H.; Ginevan, Brandon; Eck, William S.; Roebuck, Bill D.; Fishbein, James C.
Chemical Research in Toxicology, 2012 , vol. 25, # 5 p. 1022 - 1028
反应条件
pyridine; oxalyl dichloride in toluene T=20°C; Substitution; 24 h;
参考文献
Asakawa, Masumi; Brown, Christopher L.; Menzer, Stephan; Raymo, Francisco M.; Stoddart, J. Fraser; Williams, David J.
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2614 - 2627
反应条件
in dichloromethane; N,N-dimethyl-formamide
参考文献
Beacon Laboratories, Inc.
Patent: EP1216986 A2, 2002 ;
Location in patent: Page 11 ;
反应条件
sulfuric acid; copper(II) sulfate
参考文献
Eisai Co., Ltd.
Patent: EP1382603 A1, 2004 ;
Location in patent: Page 219 ;