7-甲氧基-1(2H)-异喹啉酮合成路线 （共 12 条）
反应条件
oxygen; Trimethylene glycol; copper(l) chloride; palladium dichloride in ethylene glycol dimethyl ether
参考文献
Izumi, Taeko; Nishimoto, Yasuhiro; Kohei, Kunihiro; Kasahara, Akira
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1419 - 1424
反应条件
iodine in 1,2-dichloro-benzene Heatingovernight;
参考文献
Ajao, J. F.; Bird, C. W.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 329 - 331
反应条件
1: 89 percent / tri-o-tolylphosphine, Et3N / Pd(II) acetate / acetonitrile / 24 h / 120 °C / 22800 Torr 2: 74 percent / O2, 1,3-propanediol / PdCl2, CuCl / 1,2-dimethoxy-ethane View Scheme
参考文献
Izumi, Taeko; Nishimoto, Yasuhiro; Kohei, Kunihiro; Kasahara, Akira
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1419 - 1424
反应条件
1: SOCl2 / toluene / 3 h / 80 °C 2: NaN3 / m-xylene / 5 h / 120 °C 3: 75 percent / I2 / 1,2-dichloro-benzene / Heating; overnight View Scheme
参考文献
Ajao, J. F.; Bird, C. W.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 329 - 331
反应条件
1: NaN3 / m-xylene / 5 h / 120 °C 2: 75 percent / I2 / 1,2-dichloro-benzene / Heating; overnight View Scheme
参考文献
Ajao, J. F.; Bird, C. W.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 329 - 331
参考文献
Ungnade; Nightingale; French
Journal of Organic Chemistry, 1945 , vol. 10, p. 533,534
反应条件
1: 90 percent / H2 / 10percent Pd/C / ethanol / 48 h / 80 °C / 3102.9 Torr 2: 84 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating 3: 48percent hydrobromic acid / 12 h / Heating View Scheme
参考文献
Ajao, J. F.; Bird, C. W.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 329 - 331
反应条件
1: 90 percent / H2 / 10percent Pd/C / ethanol / 48 h / 80 °C / 3102.9 Torr 2: 84 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Ajao, J. F.; Bird, C. W.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 329 - 331
反应条件
hydrogen; palladium on activated charcoal in ethanol T=80°C; P=3102.9 Torr; 48 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 329 - 331
反应条件
potassium carbonate; phosphorus oxytribromide in acetonitrile
24 h; Heating;
参考文献
Kim, Joseph T.; Gevorgyan, Vladimir
Journal of Organic Chemistry, 2005 , vol. 70, # 6 p. 2054 - 2059
