Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
triethylamine; bis(η3-allyl-μ-chloropalladium(II)) in 1,2,3,4-tetrahydro-naphthalene; water; N,N-dimethyl-formamide T=100°C; 5 h; other catalysts: (Ph3P)4Pd, LiPdCl3, (PhCN)2PdCl2, (MeCN)2PdCl2, Pd/C; Et3N absence; Further byproducts given;
参考文献
Chistovalova, N.M.; Akhrem, I.S.; Reshetova, E.V.; Vol'pin, M.E.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 10 p. 2139 - 2140
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 10 p. 2342 - 2343
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 656 - 657
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 697 - 698
in toluene Dropwise addn. of TiI4 in toluene to soln. of C(CH3)5Si(CH3)3 in toluene, stirring (2 h, color change from red to dark-red), reflux (1 h); Evapn. of solvent and byproduct (vacuum), washing of crystals (pentane), dried (vacuum), elem. anal.;
Michalski, Jan; Pakulski, Marek; Skowronska, Aleksandra
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 833 - 836
in benzene Heatingduring 5 h the solvent was distilled off, the temp. rose to 110 deg C;
参考文献
Gazizov, T. Kh.; Sudarev, Yu. I.; Shakirov, I. Kh.; Smirnov, V. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 4 p. 769 - 776,667 - 673
gallium triiodide T=140 - 170°C; 5 h; Yield givenTitle compound not separated from byproducts;
参考文献
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
gallium triiodide T=140 - 170°C; 5 h; Yield givenTitle compound not separated from byproducts;
参考文献
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
