1,1,1,3,3,3-hexamethyl-disilazane in dichloromethane
Ambient temperature;
参考文献
Rastetter, William H.; Nachbar, Robert B.; Russo-Rodriguez, Sandra; Wattley, Ruth V.; Thilly, William G.; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 25 p. 4873 - 4878
in neat (no solvent)
byproducts: Me3SnI; heating (100-110°C, 2 h); fractional distn.; product mixt. not separated;
参考文献
Bogoradovskii, E. T.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 1038 - 1039
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 1167 - 1167
Blackburn, G. Michael; Ingleson, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1150 - 1153
Shipov, A. G.; Orlova, N. A.; Savostyanova, I. A.; Artamkina, O. B.; Baukov, Yu. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 5.2 p. 1084 - 1099,959 - 971