N,N-二苯基-4-甲氧基苯甲酰胺合成路线 (共 9 条)
反应条件
pyridine in dichloromethane T=20°C; 0.0833333 h;
参考文献
Barbe, Guillaume; Charette, Andre B.
Journal of the American Chemical Society, 2008 , vol. 130, # 1 p. 18 - 19
反应条件
potassium phosphate; copper(l) iodide; N-methyl-2-(methylamino)ethylamine in toluene T=130°C; 24 h; Inert atmosphere;
参考文献
Racine, Emilie; Monnier, Florian; Vors, Jean-Pierre; Taillefer, Marc
Organic Letters, 2011 , vol. 13, # 11 p. 2818 - 2821
反应条件
in dichloromethane T=0°C; 1 h;
参考文献
Joseph, Sajan P.; Dhar, D. N.
Tetrahedron, 1986 , vol. 42, # 21 p. 5979 - 5983
反应条件
1: sodium hydrogencarbonate / dichloromethane / 1 h / 0 - 40 °C / Inert atmosphere 2: copper(l) iodide; potassium phosphate; N-methyl-2-(methylamino)ethylamine / toluene / 24 h / 130 °C / Inert atmosphere View Scheme
参考文献
Racine, Emilie; Monnier, Florian; Vors, Jean-Pierre; Taillefer, Marc
Organic Letters, 2011 , vol. 13, # 11 p. 2818 - 2821
反应条件
1: 7 percent / iodine / methanol / 31 h / 32 °C / Irradiation 2: 1.) sodium hydride / 1.) benzene, room temperature, 2.) 0 deg C, overnight View Scheme
参考文献
Datta, Indira; Das, Tapas Kumar; Ghosh, Somnath
Tetrahedron, 1990 , vol. 46, # 19 p. 6821 - 6830
反应条件
1: 7 percent / iodine / methanol / 31 h / 32 °C / Irradiation 2: 1.) sodium hydride / 1.) benzene, room temperature, 2.) 0 deg C, overnight 3: 11 percent / iodine / methanol / 30 h / 32 °C / Irradiation View Scheme
参考文献
Datta, Indira; Das, Tapas Kumar; Ghosh, Somnath
Tetrahedron, 1990 , vol. 46, # 19 p. 6821 - 6830
反应条件
iodine in methanol T=32°C; 31 h; Irradiation;
参考文献
Tetrahedron, , vol. 46, # 19 p. 6821 - 6830
反应条件
1: 7 percent / iodine / methanol / 31 h / 32 °C / Irradiation
2: 1.) sodium hydride / 1.) benzene, room temperature, 2.) 0 deg C, overnight
3: 25 percent / iodine / methanol / 25 h / 32 °C / Irradiation
View Scheme
参考文献
Datta, Indira; Das, Tapas Kumar; Ghosh, Somnath
Tetrahedron, 1990 , vol. 46, # 19 p. 6821 - 6830
反应条件
1: 7 percent / iodine / methanol / 31 h / 32 °C / Irradiation
2: 1.) sodium hydride / 1.) benzene, room temperature, 2.) 0 deg C, overnight
View Scheme
参考文献
Datta, Indira; Das, Tapas Kumar; Ghosh, Somnath
Tetrahedron, 1990 , vol. 46, # 19 p. 6821 - 6830