反应条件
1.1: nitric acid; sulfuric acid / 0 °C / |Inert atmosphere
1.2: 0 - 20 °C
1.3: 3102.97 Torr
2.1: acetonitrile / 19 h / 100 °C / |Inert atmosphere; |Reflux
3.1: trichlorophosphate; N,N-diethylaniline / 18 h / 130 °C / |Inert atmosphere
View Scheme
参考文献
Lee, Wendy; Ortwine, Daniel F.; Bergeron, Philippe; Lau, Kevin; Lin, Lichuan; Malek, Shiva; Nonomiya, Jim; Pei, Zhonghua; Robarge, Kirk D.; Schmidt, Stephen; Sideris, Steve; Lyssikatos, Joseph P.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 18 p. 5097 - 5104