[2,9,16,23-四氯-29H,31H-酞菁-N29,N30,N31,N32]合铜合成路线 （共 2 条）
反应条件
in further solvent(s) stirring of a mixt. of CuCl, urea and C8H3ClO3 in trichlorobenzene at ambient temp. for 30 minutes; heating at 175-180°C for 4 h; evapn.; heating with 5percent HCl; heating with 2percent aq. Na2CO3;; washing with H2O and ethanol; drying at 95-100°C;;
参考文献
Shigemitsu, M.
Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 691 - 693
Full Text Show Details
Gmelin Handbook: Cu: MVol.B4, 145, page 1768 - 1770
反应条件
in further solvent(s) stirring of a mixt. of Cu, urea and C8H3ClO3 in trichlorobenzene at ambient temp. for 30 minutes; heating at 175-180°C for 4 h; evapn.; heating with 5percent HCl; heating with 2percent aq. Na2CO3;; washing with H2O and ethanol; drying at 95-100°C;;
参考文献
Shigemitsu, M.
Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 691 - 693
Full Text Show Details
Gmelin Handbook: Cu: MVol.B4, 145, page 1768 - 1770
