(甲酰基甲基)磷酸二乙酯合成路线 （共 43 条）
反应条件
sodium cyanoborohydride in methanol
T=20°C; Inert atmosphere;
参考文献
Zingle, Catherine; Kuntz, Lionel; Tritsch, Denis; Grosdemange-Billiard, Catherine; Rohmer, Michel
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 21 p. 6563 - 6567,5
Title/Abstract Full Text Show Details
Zingle, Catherine; Kuntz, Lionel; Tritsch, Denis; Grosdemange-Billiard, Catherine; Rohmer, Michel
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 21 p. 6563 - 6567
反应条件
hydrogenchloride; sodium cyanoborohydride in methanol; ethanol
T=25°C; 84 h;
参考文献
Collignon, N.; Fabre, G.; Varlet, J. M.; Savignac, Ph.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 10, p. 81 - 86
反应条件
sodium cyanoborohydride
参考文献
Varlet,J.-M. et al.
Synthetic Communications, 1978 , vol. 8, p. 335 - 343
反应条件
1: 85 percent / NH2OH*HCl / ethanol; H2O / 12 h / 20 °C
2: 59 percent / triethylamine; NBS / dimethylformamide; H2O / 18 h / 20 °C
View Scheme
参考文献
Lee, Kyung Seok; Kang, Yong Koo; Yoo, Kyung Ho; Kim, Dong Chan; Shin, Kye Jung; Paik, Young-Sook; Kim, Dong Jin
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 1 p. 231 - 234
反应条件
chlorine in tetrachloromethane
T=-5 - 0°C; 2 h;
参考文献
Ismailov, V. M.; Moskva, V. V.; Dadasheva, L. A.; Zykova, T. V.; Guseinov, F. I.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 9 p. 2140 - 2141,1906
反应条件
1: 52 percent / hydroxylamine hydrochlorid, Na2CO3 / H2O / 24 h / Ambient temperature
2: N-chlorosuccinimide, pyridine / CHCl3 / 0.17 h
3: Et3N / CHCl3 / 0.5 h / Ambient temperature
View Scheme
参考文献
Nkusi, Gerard; Neidlein, Richard
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1992 , vol. 334, # 3 p. 278 - 280
反应条件
in tetrahydrofuran
1 h; Heating;
参考文献
Costisella, Burkhard; Gross, Hans
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 4 p. 143 - 144
反应条件
hydrogenchloride; sodium cyanoborohydride in methanol; ethanol
T=25°C; 120 h;
参考文献
Collignon, N.; Fabre, G.; Varlet, J. M.; Savignac, Ph.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 10, p. 81 - 86
参考文献
Oehler, Elisabeth; Kang, Heun-Soo; Zbiral, Erich
Chemische Berichte, 1988 , vol. 121, p. 299 - 308
反应条件
nitric acid; acetic anhydride
T=30°C; 1.5 h;
参考文献
Clare, Brian W.; Ferro, Vito; Skelton, Brian W.; Stick, Robert V.; White, Allan H.
Australian Journal of Chemistry, 1993 , vol. 46, # 6 p. 805 - 824
