2-(4-硝基苯基)-4H-3,1-苯并恶嗪-4-酮合成路线 (共 17 条)
反应条件
pyridine T=20°C; 0.416667 h;
参考文献
Verma, Manjusha; Singh, Sundaram; Singh
Heterocyclic Communications, 2003 , vol. 9, # 5 p. 499 - 502
反应条件
2,4,6-trichloro-1,3,5-triazine; triethylamine in toluene Heating;
参考文献
Khajavi, Mohammad S.; Shariat, Seyed M.
Heterocycles, 2005 , vol. 65, # 5 p. 1159 - 1165
反应条件
tert.-butylhydroperoxide; potassium iodide in water; acetonitrile T=80°C; 6 h;
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
反应条件
1: Et3N / CH2Cl2 / 20 °C 2: 82 percent / cyanuric chloride; Et3N / toluene / Heating View Scheme
参考文献
Khajavi, Mohammad S.; Shariat, Seyed M.
Heterocycles, 2005 , vol. 65, # 5 p. 1159 - 1165
反应条件
1: Et3N / CH2Cl2 / 20 °C 2: 82 percent / cyanuric chloride; Et3N / toluene / Heating View Scheme
参考文献
Prashanth; Revanasiddappa
Medicinal Chemistry Research, 2013 , vol. 22, # 6 p. 2665 - 2676
反应条件
oxygen in water; dimethyl sulfoxide T=20°C; pH=10.4; 6 h; Schlenk technique;
参考文献
Czaun, Miklos; Speier, Gabor; Kaizer, Jozsef; El Bakkali-Taheri, Nadia; Farkas, Etelka
Tetrahedron, 2013 , vol. 69, # 32 p. 6666 - 6672
反应条件
1: ethanol / 5 h / 20 °C 2: sodium hypochlorite / ethanol; water / 20 °C 3: tert.-butylhydroperoxide; potassium iodide / water; acetonitrile / 6 h / 80 °C View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
反应条件
1: ethanol / 5 h / 20 °C 2: sodium hypochlorite / ethanol; water / 20 °C 3: tert.-butylhydroperoxide; potassium iodide / water; acetonitrile / 6 h / 80 °C View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
反应条件
1: sodium hypochlorite / ethanol; water / 20 °C 2: tert.-butylhydroperoxide; potassium iodide / water; acetonitrile / 6 h / 80 °C View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
反应条件
1: dichloromethane / 20 h / 20 °C 2: water; sodium hydroxide / dichloromethane; methanol / |Reflux 3: thionyl chloride / 2 h / |Reflux View Scheme
参考文献
Prashanth; Revanasiddappa
Medicinal Chemistry Research, 2013 , vol. 22, # 6 p. 2665 - 2676