4'-甲氧基-[1,1'-联苯]-2-甲醛合成路线 (共 2 条)
反应条件
tert.-butylhydroperoxide; biscyclopentadienyliron(II) in decane; acetonitrile T=20 - 90°C; 24 h;
参考文献
Wertz, Sebastian; Leifert, Dirk; Studer, Armido
Organic Letters, 2013 , vol. 15, # 4 p. 928 - 931
反应条件
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 18 h / Reflux
2: pyridine / dichloromethane / 18 h / 20 °C
3: 1-(4-methoxyphenyl)ethanone / α,α,α-trifluorotoluene / 3 h / Inert atmosphere; UV-irradiation
View Scheme
参考文献
McBurney, Roy T.; Slawin, Alexandra M. Z.; Smart, Laura A.; Yu, Yanping; Walton, John C.
Chemical Communications, 2011 , vol. 47, # 28 p. 7974 - 7976