(2,6-二氯-3-硝基)苯甲醇合成路线 （共 4 条）
反应条件
sodium tetrahydroborate in methanol T=10°C; 1 h;
参考文献
Abe, Yoshito; Kayakiri, Hiroshi; Satoh, Shigeki; Inoue, Takayuki; Sawada, Yuki; Imai, Keisuke; Inamura, Noriaki; Asano, Masayuki; Hatori, Chie; Katayama, Akira; Oku, Teruo; Tanaka, Hirokazu
Journal of Medicinal Chemistry, 1998 , vol. 41, # 4 p. 564 - 578
反应条件
borane-THF in tetrahydrofuran 48 h; Heating / reflux;
参考文献
US2005/250796 A1, ;
Page/Page column 13 ;
反应条件
1: 81.5 percent / imidazole / dimethylformamide / 3 h / Ambient temperature 2: FeCl3*6H2O, C, NH2-NH2*H2O / methanol; H2O / 5 h / 70 °C View Scheme
参考文献
Abe, Yoshito; Kayakiri, Hiroshi; Satoh, Shigeki; Inoue, Takayuki; Sawada, Yuki; Inamura, Noriaki; Asano, Masayuki; Aramori, Ichiro; Hatori, Chie; Sawai, Hiroe; Oku, Teruo; Tanaka, Hirokazu
Journal of Medicinal Chemistry, 1998 , vol. 41, # 21 p. 4062 - 4079
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
T=20°C; 6 h;
参考文献
Yamada, Tatsuhiro; Nakagawa, Tadakiyo; Tanaka, Yasuhiro; Fujita, Kohichi; Tagami, Tomoyuki; Ikenoue, Yuka; Fukuda, Shunsuke; Chujo, Yoshitomo; Suzuki, Manabu; Murata, Masahiro
Patent: US2005/250796 A1, 2005 ;
Location in patent: Page/Page column 13 ;
