2,2-二氯-3-氧代-3-苯基丙烷醛合成路线 （共 16 条）
反应条件
chlorine in tetrachloromethane T=20 - 30°C; 1 h;
参考文献
Guseinov, F. I.; Moskva, V. V.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 3.1 p. 384 - 390
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 3 p. 360 - 365
反应条件
in benzene T=40 - 45°C; 24 h;
参考文献
Guseinov; Klimentova; Egereva; Moskva
Russian Journal of General Chemistry, 1996 , vol. 66, # 6 p. 952 - 957
反应条件
sodium methylate in diethyl ether 1 h; Ambient temperature;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 1.2 p. 86 - 89
Zhurnal Organicheskoi Khimii, , vol. 31, # 1 p. 96 - 99
反应条件
1-amino-2,4-dimethylbenzene in tetrachloromethane 12 h; Ambient temperature;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 4 p. 530 - 533
Zhurnal Organicheskoi Khimii, , vol. 30, # 4 p. 496 - 499
反应条件
in tetrachloromethane 12 h; Ambient temperature;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 4 p. 530 - 533
Zhurnal Organicheskoi Khimii, , vol. 30, # 4 p. 496 - 499
反应条件
in diethyl ether 1.) -20 deg C, 1 h, 2.) room temperature, 4 h;
参考文献
Guseinov; Burangulova; Moskva
Russian Journal of General Chemistry, 1997 , vol. 67, # 10 p. 1564 - 1567
反应条件
diethyl sodium phosphite in diethyl ether T=-20°C; 1 h;
参考文献
Guseinov; Burangulova; Ismailov
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 5 p. 742 - 743
反应条件
1-amino-2,4-dimethylbenzene in tetrachloromethane 12 h; Ambient temperature;
参考文献
Guseinov, F. I.; Klimentova, G. Yu.; Moskva, V. V.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 4 p. 530 - 533
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 4 p. 496 - 499
反应条件
1: acetylacetone With sodium hydride in diethyl ether Metallation; 1 h; Heating; 2: benzoyl(dichloro)acetaldehyde in diethyl ether T=20°C; Formylation; elimination;
参考文献
Guseinov, F. I.
Russian Chemical Bulletin, 1999 , vol. 48, # 4 p. 743 - 745
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1999 , # 4 p. 747 - 749
反应条件
1,2-diamino-benzene in tetrachloromethane 1.) -5 deg C to 0 deg C, 1 h, 2.) 20 deg C, 1 h;
参考文献
Guseinov; Klimentova; Yudina; Kol'tsova; Moskva
Russian Chemical Bulletin, 1998 , vol. 47, # 3 p. 459 - 461
