1,2-双(三乙氧基硅基)乙烷合成路线 （共 20 条）
反应条件
1: in toluene T=50 - 60°C; 1 h; Inert atmosphereReflux; 2: With hydrogen; palladium 10 on activated carbon in ethanol T=80°C; P=3750.38 Torr; 4 h;
参考文献
US2012/123143 A1, ;
Page/Page column 3 ;
反应条件
hydrogen; palladium 10 on activated carbon in ethanol P=750.075 Torr; 1 h;
参考文献
US2012/123143 A1, ;
Page/Page column 4 ;
反应条件
Platinum catalyst II T=110 - 120°C; 7 h;
参考文献
Pomerantseva, M. G.; Belyakova, Z. V.; Shchepinov, S. A.; Efimova L. A.; Chernyshev, E. A.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 2 p. 354 - 356,316 - 318
反应条件
[Pt(triphenylphosphine)2Cl2] in benzene T=80°C; 10 h; other hydrosilanes; var. group-VIII metal phosphine complexes as catalysts, var. solvents, var. conc., var. temperatures and times; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 195, # 3 p. 363 - 374
反应条件
in dichloromethane T=50°C; 0.5 h;
参考文献
Lakhtin; Nosova; Kisin; Ivanov; Chernyshev
Russian Journal of General Chemistry, 2001 , vol. 71, # 8 p. 1252 - 1254
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I) T=45°C; 2 h;
参考文献
Voronkov, M. G.; Pukhnarevich, V. B.; Tsykhanskaya, I. I.; Varshavskii, Yu. S.
Doklady Chemistry, 1980 , vol. 254, p. 449 - 451
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 254, # 4 p. 887 - 890
反应条件
Rh(I)-catalyst in tetrahydrofuran 1 h; Ambient temperature; Yields of byproduct given;
参考文献
Brockmann, Monika; Dieck, Heindirk tom; Klaus, Juergen
Journal of Organometallic Chemistry, 1986 , vol. 301, p. 209 - 226
反应条件
Ru(acac)2 2 h; Heating;
参考文献
Polish Journal of Chemistry, , vol. 56, # 2 p. 287 - 296
反应条件
aluminium trichloride T=110 - 120°C; 3 h;
参考文献
Zhun; Sbitneva; Polivanov; Chernyshev
Russian Journal of General Chemistry, 2006 , vol. 76, # 10 p. 1564 - 1570
反应条件
bis(acetylacetonate)nickel(II); tri-cyclo-hexyl-phosphine T=120°C; 40 h; Further byproducts given;
参考文献
Journal of Organometallic Chemistry, , vol. 484, # 1-2 p. 147 - 152
