1-叠氮基-1,2-苯并氧代-3(1h)-酮合成路线 （共 4 条）
反应条件
trimethylsilyl trifluoromethanesulfonate; trifluoromethanesulfonyl azide in dichloromethane
0.5 h; Inert atmosphere;
参考文献
Fan, Yunpeng; Wan, Wen; Ma, Guobin; Gao, Wei; Jiang, Haizhen; Zhu, Shizheng; Hao, Jian
Chemical Communications, 2014 , vol. 50, # 43 p. 5733 - 5736
反应条件
trimethylsilylazide in acetonitrile
15 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Krasutsky, Alexei P.; Kuehl, Chris J.; Simonsen, Angela J.; Woodward, Jessica K.; Mismash, Brian; Bolz, Jason T.
Journal of the American Chemical Society, 1996 , vol. 118, # 22 p. 5192 - 5197
反应条件
trimethylsilylazide in acetonitrile
Ambient temperature;
参考文献
Zhdankin, Viktor V.; Kuehl, Chris J.; Krasutsky, Alexei P.; Formaneck, Mark S.; Bolz, Jason T.
Tetrahedron Letters, 1994 , vol. 35, # 52 p. 9677 - 9680
反应条件
1: sodium periodate; acetic acid / water / 4 h / |Reflux
2: |Reflux; |Inert atmosphere
3: trimethylsilylazide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Vita, Maria Victoria; Waser, Jerome
Organic Letters, 2013 , vol. 15, # 13 p. 3246 - 3249
