4-[[[(1,1-二甲基乙基)二甲基甲硅烷基]氧基]甲基]苯甲醛合成路线 （共 14 条）
反应条件
1: 3M aq. HCl / tetrahydrofuran / 6 h / 25 °C 2: imidazole / acetonitrile / 8 h / 25 °C View Scheme
参考文献
Barluenga; Del Pozo; Olano
Synthesis, 1995 , # 12 p. 1529 - 1533
反应条件
1: TsOH / benzene / 14 h / Heating 2: LiAlH4 / diethyl ether / 1 h / 0 °C 3: 3M aq. HCl / tetrahydrofuran / 6 h / 25 °C 4: imidazole / acetonitrile / 8 h / 25 °C View Scheme
参考文献
Barluenga; Del Pozo; Olano
Synthesis, 1995 , # 12 p. 1529 - 1533
反应条件
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 4 h 2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -70 °C 2.2: 4 h / -70 - -5 °C View Scheme
参考文献
KATHOLIEKE UNIVERSITEIT LEUVEN; BARDIOT, Dorothée; CARLENS, Gunter; DALLMEIER, Kai; KAPTEIN, Suzanne; McNAUGHTON, Michael; MARCHAND, Arnaud; NEYTS, Johan; SMETS, Wim
Patent: WO2013/45516 A1, 2013 ;
反应条件
[bis(3-methylimidazole-3-ium) tetraethylene glycol] dimesylate in methanol T=20°C; 1.33333 h;
参考文献
Jadhav, Arvind H.; Kim, Hern
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5338 - 5342
