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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
160750-61-8
合成路线
（共 13 条）
594858-64-7
→
反应条件
160750-61-8
反应条件
Grubb's 2nd generation catalyst in dichloromethane T=25°C; 5 h;
参考文献
Clavier, Herve; Nolan, Steven P.
Chemistry - A European Journal, 2007 , vol. 13, # 28 p. 8029 - 8036
594858-64-7
→
反应条件
1400471-16-0
反应条件
Grubb's 2nd generation catalyst; iron in toluene T=100°C; 3 h; Inert atmosphere;
参考文献
Wang, Jianhui; Shao, Mingbo; Zheng, Lu; Qiao, Weixia; Wang, Jingjing
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2743 - 2750,8
594858-64-7
→
反应条件
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene); iron in toluene T=100°C; 3 h; Inert atmosphere;
参考文献
Wang, Jianhui; Shao, Mingbo; Zheng, Lu; Qiao, Weixia; Wang, Jingjing
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2743 - 2750,8
255043-71-1
→
反应条件
160750-61-8
反应条件
α-n-hexadecene; (H2IMes)[(C6F13-CH2CH2)3P](Cl2)Ru(=CHPh) in dichloromethane T=20°C; 1 h;
参考文献
Da Costa, Rosenildo Correa; Gladysz, John A.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 1-2 p. 243 - 254
50487-71-3
N-烯丙基对甲苯磺酰胺
→
反应条件
160750-61-8
反应条件
1: 80 percent / sodium hydride / dimethylformamide; various solvent(s) / 16 h / 20 °C 2: 77 percent / first generation Grubbs' catalyst / CH2Cl2 / 2 h / Heating 3: 99 percent Spectr. / triethylamine; formic acid; tri-n-butylphosphine / allylpalladium chloride dimer / dimethylformamide / 21 h / 60 °C View Scheme
参考文献
Schmidt, Bernd; Krehl, Stefan; Jablowski, Eric
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 26 p. 5119 - 5130
935553-10-9
→
反应条件
160750-61-8
反应条件
formic acid; tributylphosphine; triethylamine; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=60°C; 21 h;
参考文献
Cheng, Hsiu-Yi; Sun, Chong-Si; Hou, Duen-Ren
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2674 - 2677
55962-05-5
+
78-79-5
异戊二烯
→
反应条件
160750-61-8
反应条件
Cu(1,1,1,5,5,5-hexafluoroacetylacetonate)2 in chlorobenzene T=25°C; 24 h; Inert atmosphere;
参考文献
Wu, Qiong; Hu, Jian; Ren, Xinfeng; Zhou, Jianrong
Chemistry - A European Journal, 2011 , vol. 17, # 41 p. 11553 - 11558
594858-64-7
→
反应条件
153633-33-1
+
160750-61-8
反应条件
1: With Grubb's 2nd generation catalyst in toluene T=80°C; 0.5 h; Inert atmosphere; 2: With tert.-butylhydroperoxide in decane; toluene T=20°C; 0.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Krehl, Stefan; Jablowski, Eric
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 26 p. 5119 - 5130
120702-33-2
→
反应条件
160750-61-8
反应条件
1: 77 percent / first generation Grubbs' catalyst / CH2Cl2 / 2 h / Heating 2: 99 percent Spectr. / triethylamine; formic acid; tri-n-butylphosphine / allylpalladium chloride dimer / dimethylformamide / 21 h / 60 °C View Scheme
参考文献
Cheng, Hsiu-Yi; Sun, Chong-Si; Hou, Duen-Ren
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2674 - 2677
98-59-9
对甲苯磺酰氯
→
反应条件
160750-61-8
反应条件
1.1: dichloromethane / 12 h / 20 °C / Inert atmosphere 2.1: potassium carbonate / acetonitrile / 12 h / 60 °C / Inert atmosphere 3.1: Grubb's 2nd generation catalyst / toluene / 0.5 h / 80 °C / Inert atmosphere 3.2: 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Schmidt, Bernd; Krehl, Stefan; Jablowski, Eric
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 26 p. 5119 - 5130
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