iodine; isopentyl nitrite in 1,4-dioxane; chloroform-d1 18 h; Heating;

bis(triphenylphosphine)palladium(II)-chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl acetamide T=115°C; P=4654.3 - 4912.9 Torr; 4 h;