2-(4-氟亚苄基)苯乙酮合成路线 (共 22 条)
反应条件
1: 59 percent / CH2Cl2 / 40 - 42 °C 2: 57 percent / KOH / ethanol / Heating View Scheme
参考文献
Prakash, Om; Kumar, Rajesh; Sharma, Deepak; Pannu, Kamaljeet; Kamal, Raj
Synlett, 2007 , # 14 p. 2189 - 2192
反应条件
aluminum oxide; Bi(NO3)3 T=130°C;
参考文献
Kumar, Anil; Koul, Summon; Razdan, Tej K.; Kapoor, Kamal K.
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 837 - 842
反应条件
urea; Bi(NO3)3/ZnCl2 on Al2O3 in chloroform
T=130°C; 0.383333 h; microwave irradiation;
参考文献
Verma, Anil K.; Koul, Summon; Pannu, Ajay P.S.; Razdan, Tej K.
Tetrahedron, 2007 , vol. 63, # 36 p. 8715 - 8722
反应条件
urea; aluminum oxide; Bi(NO3)3
T=130°C;
参考文献
Kumar, Anil; Koul, Summon; Razdan, Tej K.; Kapoor, Kamal K.
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 837 - 842
反应条件
aluminum oxide; Bi(NO3)3
T=130°C;
参考文献
Kumar, Anil; Koul, Summon; Razdan, Tej K.; Kapoor, Kamal K.
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 837 - 842
参考文献
ORION CORPORATION
Patent: EP1261588 B1, 2004 ;
EP 1261588 B1
参考文献
Huhtala, Paavo; Karjalainen, Arto; Haapalinna, Antti; Lehtimaki, Jyrki; Karjalainen, Arja; Virtanen, Raimo
Patent: US2001/56109 A1, 2001 ;
反应条件
morpholine; sulfur in ethanol
Condensation; thiolation, cyclization; Heating;
参考文献
Shestopalov; Nikishin
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 9 p. 1093 - 1093
反应条件
1: 83 percent / ethanol
2: 38 percent / O2 / acetic acid / 0.5 h / Heating
View Scheme
参考文献
Krauze, A. A.; Kalme, Z. A.; Pelcher, Yu. E.; Liepin'sh, E. E.; Dipan, I. V.; Dubur, G. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1202 - 1207
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1515 - 1520
反应条件
1: piperidine / ethanol / 6 h / Reflux
2: potassium hydroxide / ethanol / 24 h / 30 °C
View Scheme
参考文献
Mishriky; Girgis; Ahmed-Farag
Egyptian Journal of Chemistry, 2009 , vol. 52, # 2 p. 249 - 264