4-氟-3-(甲基磺酰基)苯甲酸甲酯合成路线 (共 5 条)
反应条件
in water; N,N-dimethyl-formamide
参考文献
Hoechst Aktiengesellschaft
Patent: US6057322 A1, 2000 ;
反应条件
1: ClSO3H / 6 h / 140 °C 2: aq. Na2SO3, aq. NaOH / 15 - 20 °C 3: K2CO3 / dimethylformamide / Ambient temperature View Scheme
参考文献
Baumgarth, Manfred; Beier, Norbert; Gericke, Rolf
Journal of Medicinal Chemistry, 1997 , vol. 40, # 13 p. 2017 - 2034
反应条件
1: aq. Na2SO3, aq. NaOH / 15 - 20 °C 2: K2CO3 / dimethylformamide / Ambient temperature View Scheme
参考文献
Baumgarth, Manfred; Beier, Norbert; Gericke, Rolf
Journal of Medicinal Chemistry, 1997 , vol. 40, # 13 p. 2017 - 2034
反应条件
potassium carbonate in N,N-dimethyl-formamide Ambient temperature; Yield given;
参考文献
Baumgarth, Manfred; Beier, Norbert; Gericke, Rolf
Journal of Medicinal Chemistry, 1997 , vol. 40, # 13 p. 2017 - 2034
参考文献
Hoechst Aktiengesellschaft
Patent: US6057322 A1, 2000 ;