[6,6]-苯基 C61 丁酸甲酯合成路线 (共 4 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in 1,2-dichloro-benzene T=20°C; 6 h; Reagent/catalystSolventTemperature;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Matsumoto, Fukashi; Hida, Koichi; Moriwaki, Kazuyuki; Takao, Yuko; Mizuno, Takumi; Ohno, Toshinobu
Synlett, 2013 , vol. 24, # 15 art. no. ST-2013-U0436-L, p. 1988 - 1992
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in 1,2-dichloro-benzene T=20°C; 6 h;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Matsumoto, Fukashi; Hida, Koichi; Moriwaki, Kazuyuki; Takao, Yuko; Mizuno, Takumi; Ohno, Toshinobu
Synlett, 2013 , vol. 24, # 15 art. no. ST-2013-U0436-L, p. 1988 - 1992
反应条件
pyridine; sodium methylate in 1,2-dichloro-benzene T=65 - 70°C; 24 h;
参考文献
Zheng, Liping; Zhou, Qingmei; Deng, Xianyu; Yuan, Min; Yu, Gang; Cao, Yong
Journal of Physical Chemistry B, 2004 , vol. 108, # 32 p. 11921 - 11926
反应条件
2,2,6,6-tetramethyl-piperidine; toluene-4-sulfonic acid hydrazide in 1,2-dichloro-benzene T=70 - 250°C; Inert atmosphereContinuous flow reactor;
参考文献
Seyler, Helga; Wong, Wallace W. H.; Jones, David J.; Holmes, Andrew B.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3551 - 3556