1,4-二甲基-1H-吡唑-5-甲酰氯合成路线 (共 5 条)
反应条件
1: 92 percent / 1 N aq. NaOH / ethanol / 2 h / Heating 2: SOCl2 / 2 h / Heating View Scheme
参考文献
Huppatz; Phillips; Witrzens
Agricultural and Biological Chemistry, 1984 , vol. 48, # 1 p. 45 - 50
反应条件
1: 30 percent / NaOEt / ethanol / Ambient temperature 2: 92 percent / 1 N aq. NaOH / ethanol / 2 h / Heating 3: SOCl2 / 2 h / Heating View Scheme
参考文献
Huppatz; Phillips; Witrzens
Agricultural and Biological Chemistry, 1984 , vol. 48, # 1 p. 45 - 50
反应条件
thionyl chloride 2 h; Heating;
参考文献
Huppatz; Phillips; Witrzens
Agricultural and Biological Chemistry, 1984 , vol. 48, # 1 p. 45 - 50
参考文献
Rojahn; Kuehling
Archiv der Pharmazie (Weinheim, Germany), 1926 , p. 346
反应条件
pyridine
0.5 h; Heating; Yield given;
参考文献
Huppatz; Phillips; Witrzens
Agricultural and Biological Chemistry, 1984 , vol. 48, # 1 p. 45 - 50