1.1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice
1.2: 4 h / Inert atmosphere; Reflux
2.1: hydrogen / ethanol / 10 h / 85 °C / 30003 Torr / Autoclave
View Scheme
参考文献
Yu, Fabiao; Li, Peng; Li, Guangyue; Zhao, Guangjiu; Chu, Tianshu; Han, Keli
Journal of the American Chemical Society, 2011 , vol. 133, # 29 p. 11030 - 11033
1.1: selenium / diethyl ether / 0.5 h / Reflux
1.2: Cooling with ice
2.1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice
2.2: 4 h / Inert atmosphere; Reflux
3.1: hydrogen / ethanol / 10 h / 85 °C / 30003 Torr / Autoclave
View Scheme
参考文献
Yu, Fabiao; Li, Peng; Li, Guangyue; Zhao, Guangjiu; Chu, Tianshu; Han, Keli
Journal of the American Chemical Society, 2011 , vol. 133, # 29 p. 11030 - 11033