全氟(4-甲基-3,6-二氧杂-7-辛烯)磺酰氟合成路线 （共 4 条）
4089-58-12,3,3,3-四氟-2-[1,1,2,3,3,3-六氟-2-[1,1,2,2-四氟-2-(氟磺酰基)乙氧基]丙氧基]丙酰氟
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反应条件
sodium carbonate T=220°C;
参考文献
Hoshi, Nobuto; Uematsu, Nobuyuki; Ikeda, Masanori
Patent: US2004/176636 A1, 2004 ;
Location in patent: Page 7 ;
反应条件
1: With cesium fluoride in various solvent(s) T=-15°C; P=750 Torr; 8 h; 2: With sodium carbonate T=210 - 225°C; 4 h;
参考文献
Thomas, Brian H.; Shafer, Gregory; Ma, Jing Ji; Tu, Ming-Hu; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 8 p. 1231 - 1240
反应条件
sodium carbonate molar ratio of educts = 2:1, vigorous stirring, 8 h, 160-170°C; by-product is removed by heating to 300°C;
参考文献
DE2128256 , ;
C.A., , vol. 76, p. 58973
反应条件
T=185 - 240°C; 12 h;
参考文献
Yang, Zhen-Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2394 - 2403
