反应条件
1: 40 percent / aq. H2SO4 / 25 °C / controlled potential electrochem. reduction, (-)Hg/Pt(+), -1000 mV vs. s.c.e.
2: 30 percent / 1-hydroxy-benzotriazole, 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH2Cl2 / 2 h, 0 deg C; 2 h, 20 deg C
View Scheme
参考文献
Largeron, M.; Vuilhorgne, M.; Potier, I. Le; Auzeil, N.; Bacque, E.; and al.
Tetrahedron, 1994 , vol. 50, # l p. 6307 - 6332
