1,6-己二醇二缩水甘油醚合成路线 （共 6 条）
反应条件
tetrabutyl-ammonium chloride; sodium hydroxide in water T=40°C; 2 h;
参考文献
Yi, Wen-Jing; Feng, Zhi-Hua; Zhang, Qin-Fang; Zhang, Ji; Li, Ling-Dong; Zhu, Wen; Yu, Xiao-Qi
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2413 - 2421
反应条件
dihydrogen peroxide; benzonitrile; triethylamine in water T=60°C; 25 h; Conversion of starting material;
参考文献
US2012/29217 A1, ;
Page/Page column 6-7 ;
反应条件
sodium hydride in hexane; toluene T=20°C; Cyclization; 0.0833333 h;
参考文献
Van Elburg; Ormskerk; De Kloe; Boogaard
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 2 p. 147 - 167
反应条件
1: SnCl4 / toluene; heptane / 3 h / 90 °C 2: 228 mg / NaH / toluene; hexane / 0.08 h / 20 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 43, # 2 p. 147 - 167
反应条件
potassium hydroxide in tetrahydrofuran 5 h; Heating;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 74, # 3 p. 235 - 240
反应条件
potassium hydroxide in tetrahydrofuran 7 h; Heating;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 74, # 3 p. 235 - 240
