4,6-邻亚苄基-1-硫代-b-甲基葡萄糖甙-4-甲基苯酯合成路线 （共 6 条）
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=50°C; 0.0223333 h;
参考文献
Vargas-Berenguel, Antonio; Meldal, Morten; Paulsen, Hans; Jensen, Knud J.; Bock, Klaus
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 22 p. 3287 - 3294
反应条件
toluene-4-sulfonic acid in acetonitrile T=20°C; 5 h;
参考文献
Dhenin, Sandrine G.Y.; Moreau, Vincent; Morel, Nathalie; Nevers, Marie-Claire; Volland, Herve; Creminon, Christophe; Djedaini-Pilard, Florence
Carbohydrate Research, 2008 , vol. 343, # 12 p. 2101 - 2110
反应条件
1: 80 percent / BF3*Et2O / CH2Cl2 2: 99 percent / NaOMe / methanol 3: 81 percent / DL-10-camphorsulfonic acid / acetonitrile View Scheme
参考文献
Vargas-Berenguel, Antonio; Meldal, Morten; Paulsen, Hans; Jensen, Knud J.; Bock, Klaus
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 22 p. 3287 - 3294
反应条件
1: 80 percent / BF3*Et2O / CH2Cl2 2: 99 percent / NaOMe / methanol 3: 81 percent / DL-10-camphorsulfonic acid / acetonitrile View Scheme
参考文献
Vargas-Berenguel, Antonio; Meldal, Morten; Paulsen, Hans; Jensen, Knud J.; Bock, Klaus
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 22 p. 3287 - 3294
反应条件
1: 99 percent / NaOMe / methanol 2: 81 percent / DL-10-camphorsulfonic acid / acetonitrile View Scheme
参考文献
Wang, Changning; Li, Qin; Wang, Haisheng; Zhang, Li-He; Ye, Xin-Shan
Tetrahedron, 2006 , vol. 62, # 50 p. 11657 - 11662
反应条件
tetra-(n-butyl)ammonium iodide; sodium hydride in N,N-dimethyl-formamide T=65 - 70°C; 1 h;
参考文献
US2011/224158 A1, ;
Page/Page column 17-18 ;
