十四甲基-1,11-二氯六硅氧烷合成路线 （共 6 条）
反应条件
water in 1,4-dioxane; diethyl ether; water addn. of H2O (8.3 mol) in dioxane to a soln. of (CH3)2SiCl2 (16.6 mol) in ether;;
参考文献
Patnode, W. I.; Wilcock, D. F.
Journal of the American Chemical Society, 1946 , vol. 68, p. 358 - 363
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 104, page 286 - 288
Full Text Show Details
General Electric Co.
Patent: US2381366 , 1945 ;
C. A., 1945 , p. 4890
反应条件
1,4-dioxane; diethyl ether; water
参考文献
Gen.Electric Co.
Patent: US2421653 , 1944 ;
反应条件
aluminium trichloride in neat (no solvent) ((CH3)2SiO)4 and AlCl3 at about 120°C;;
参考文献
Gmelin Handbook: Si: MVol.C, 104, page 286 - 288
反应条件
triethylamine in diethyl ether 1 h; Heating;
参考文献
Sonnek, Georg; Engelbrecht, Lothar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 9 p. 343 - 344
反应条件
triethylamine in diethyl ether 1 h; Heating;
参考文献
Sonnek, Georg; Engelbrecht, Lothar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 9 p. 343 - 344
反应条件
sodium hydroxide in diethyl ether
参考文献
Andrianov,K.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , p. 2144 - 2146
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , p. 2243 - 2245
