N-羟乙基-3,3-二甲基-6-硝基吲哚啉螺吡喃合成路线 (共 9 条)
反应条件
in ethanol 3 h; Heating;
参考文献
Raymo; Giordani
Journal of the American Chemical Society, 2001 , vol. 123, # 19 p. 4651 - 4652
反应条件
1: 1-(2-hydroxyethyl)-2,3,3-trimethyl-3H-indolium bromide With potassium hydroxide T=20°C; 0.5 h; 2: 2-hydroxy-5-nitro-benzaldehyde in ethanol 6 h; RefluxInert atmosphere;
参考文献
Natali, Manuel; Giordani, Silvia
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 6 p. 1162 - 1171
反应条件
1: 2,3,3-trimethyl-(3H)-indoleine; 2-bromo-1-ethanol in acetonitrile 24 h; RefluxInert atmosphere; 2: With potassium hydroxide in water T=20°C; 0.5 h; 3: 2-hydroxy-5-nitro-benzaldehyde in ethanol 3 h; RefluxInert atmosphere;
参考文献
Zhu, Ming-Qiang; Zhang, Guo-Feng; Hu, Zhe; Aldred, Matthew P.; Li, Chong; Gong, Wen-Liang; Chen, Tao; Huang, Zhen-Li; Liu, Shiyong
Macromolecules, 2014 , vol. 47, # 5 p. 1543 - 1552
反应条件
1: 61 percent / xylene / 0.25 h / Ambient temperature; Irradiation 2: 88 percent / piperidine / ethanol / 0.17 h / Ambient temperature; Irradiation View Scheme
参考文献
Synthetic Communications, , vol. 28, # 21 p. 4035 - 4041
反应条件
piperidine in ethanol 0.166667 h; Ambient temperatureIrradiation;
参考文献
Gonzalez De Los S, Eduardo A.; Lozano G, Ma. Josefina
Synthetic Communications, 1998 , vol. 28, # 21 p. 4035 - 4041
参考文献
May, Florian; Peter, Michael; Huetten, Andreas; Prodi, Luca; Mattay, Jochen
Chemistry - A European Journal, 2012 , vol. 18, # 3 p. 814 - 821
反应条件
in acetonitrile T=24.85°C; Equilibrium constantKinetics;
参考文献
Journal of Organic Chemistry, , vol. 68, # 11 p. 4158 - 4169
反应条件
1: NaOH / H2O 2: ethanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 20 p. 5377 - 5383
反应条件
bis(4'-(4-pyridyl)-2,2':6',6''-terpyridine)ruthenium(II) in acetonitrile Irradiation;
参考文献
Chemistry - A European Journal, , vol. 15, # 1 p. 178 - 185