磷腈配体P1-叔丁基三(亚甲基)合成路线 (共 3 条)
反应条件
1: T=5 - 85°C; Inert atmosphere; 2: With BaO T=140°C; 40 h; Inert atmosphere;
参考文献
Boltukhina, Ekaterina V.; Sheshenev, Andrey E.; Lyapkalo, Ilya M.
Tetrahedron, 2011 , vol. 67, # 30 p. 5382 - 5388
反应条件
potassium hydroxide 1.) -40 deg C to 80 deg C; reflux, 2 h;
参考文献
Schwesinger, Reinhard; Willaredt, Juergen; Schlemper, Helmut; Keller, Manfred; Schmitt, Dieter; Fritz, Hans
Chemische Berichte, 1994 , vol. 127, # 12 p. 2435 - 2454
反应条件
1: 0 - 20 °C 2: 36 h / 145 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 9 p. 1811 - 1823