2-(4-甲基苯基)苯并噻唑合成路线 (共 67 条)
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
反应条件
in toluene T=20°C; 1.5 h; Green chemistry;
参考文献
Sung, Gi Hyeon; Lee, In-Hye; Kim, Bo Ram; Shin, Dong-Soo; Kim, Jeum-Jong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Tetrahedron, 2013 , vol. 69, # 17 p. 3530 - 3535
反应条件
((C6H4)(PPh2)(NCHPhP(O)Ph2))NiCl in diethyl ether T=25°C; Kumada cross-coupling; 12 h; Inert atmosphere;
参考文献
Liu, Ning; Wang, Zhong-Xia
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10031 - 10038
反应条件
Pd0(tris(tert-butyl)phosphine)2; lithium tert-butylate in 1,4-dioxane T=100°C; Inert atmosphere; regioselective reaction;
参考文献
Tamba, Shunsuke; Okubo, Youhei; Tanaka, Shota; Monguchi, Daiki; Mori, Atsunori
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 6998 - 7001
反应条件
PhCH2Pd(PPh3)2Cl; Cu(I) 3-methylsalicylate in tetrahydrofuran T=50°C; 14 h;
参考文献
Egi, Masahiro; Liebeskind, Lanny S
Organic letters, 2003 , vol. 5, # 6 p. 801 - 802
反应条件
copper diacetate; palladium diacetate; triphenylphosphine in 1,4-dioxane; dimethyl sulfoxide T=120°C; 24 h; Inert atmosphere;
参考文献
Liu, Bo; Li, Jian; Song, Feijie; You, Jingsong
Chemistry - A European Journal, 2012 , vol. 18, # 35 p. 10830 - 10833
反应条件
copper diacetate; triethylamine in ethanol T=70°C; 6 h;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Wu, Xia
Organic Letters, 2013 , vol. 15, # 7 p. 1598 - 1601
反应条件
Dess-Martin periodane in dichloromethane T=20°C;
参考文献
Bose, D. Subhas; Idrees, Mohd.
Synthesis, 2010 , # 3 p. 398 - 402
反应条件
oxygen; copper(l) chloride; lithium tert-butylate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 0.166667 h;
参考文献
Yang, Fanzhi; Xu, Zhaoqing; Wang, Zhe; Yu, Zhengkun; Wang, Rui
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6321 - 6325
反应条件
magnesium sulfate; copper(l) chloride in dimethyl sulfoxide T=110°C; 6 h;
参考文献
Park, Namjin; Heo, Yumi; Kumar, Manian Rajesh; Kim, Yong; Song, Kwang Ho; Lee, Sunwoo
European Journal of Organic Chemistry, 2012 , # 10 p. 1984 - 1993