4,6-二甲基-2-羟基吡啶合成路线 (共 30 条)
参考文献
Journal of the Chemical Society, , vol. 81, p. 116
反应条件
1: Br2; acetic acid / 1 h 2: 79 percent / POCl3 / 8 h / 135 °C 3: Na2CO3 / Pd(PPh3)4 / toluene; H2O; ethanol / 8 h / 105 °C View Scheme
参考文献
Synthesis, , # 17 p. 2855 - 2864
参考文献
Journal of the Chemical Society, , vol. 71, p. 303
Chemische Berichte, , vol. 20, p. 446
反应条件
1: Br2; acetic acid / 1 h 2: 79 percent / POCl3 / 8 h / 135 °C 3: 83 percent / aq. HI; phosphorus / 16 h / Heating View Scheme
参考文献
Blachut, Dariusz; Czarnocki, Zbigniew; Wojtasiewicz, Krystyna
Synthesis, 2006 , # 17 p. 2855 - 2864
反应条件
1: Br2; acetic acid / 1 h 2: 79 percent / POCl3 / 8 h / 135 °C 3: 83 percent / aq. HI; phosphorus / 16 h / Heating 4: K2CO3 / Pd(PPh3)4 / 1,2-dimethoxy-ethane; H2O / 24 h / 75 °C View Scheme
参考文献
Blachut, Dariusz; Czarnocki, Zbigniew; Wojtasiewicz, Krystyna
Synthesis, 2006 , # 17 p. 2855 - 2864
参考文献
Journal of the Chemical Society, , vol. 71, p. 303
Chemische Berichte, , vol. 20, p. 446
参考文献
Collie
Journal of the Chemical Society, 1897 , vol. 71, p. 303
Chemische Berichte, 1887 , vol. 20, p. 446
反应条件
sodium methylate in methanol
12 h; Heating;
参考文献
Tohda; Kawahara; Eiraku; Tani; Nisiwaki; Ariga
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 8 p. 2176 - 2186
参考文献
Hantzsch
Chemische Berichte, 1884 , vol. 17, p. 2904
反应条件
sodium hydroxide; cis amino chloride; water
unter Kuehlung;
参考文献
Hoegerle
Helvetica Chimica Acta, 1958 , vol. 41, p. 548,553