(4-溴苯基乙炔基)三甲基硅烷合成路线 （共 34 条）
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine T=0°C; Schlenk techniqueInert atmosphere;
参考文献
Marques-Gonzalez, Santiago; Yufit, Dmitry S.; Howard, Judith A.K.; Martin, Santiago; Osorio, Henrry M.; Garcia-Suarez, Victor M.; Nichols, Richard J.; Higgins, Simon J.; Cea, Pilar; Low, Paul J.
Dalton Transactions, 2013 , vol. 42, # 2 p. 338 - 341
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran T=20°C; Hagihara-Sonogashira coupling; 18 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 5 p. 946 - 953
反应条件
zinc trifluoromethanesulfonate; triethylamine in dichloromethane T=23°C; 12 h;
参考文献
Rahaim Jr., Ronald J.; Shaw, Jared T.
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2912 - 2915
反应条件
chloro-trimethyl-silane in tetrahydrofuran; methanol
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine T=20°C; Sonogashira coupling reaction;
参考文献
Huang, Chun; Zhen, Chang-Gua; Siew, Ping Su; Kian, Ping Loh; Chen, Zhi-Kuan
Organic Letters, 2005 , vol. 7, # 3 p. 391 - 394
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran T=20°C; Sonogashira Cross-Coupling; Inert atmosphereSealed tube;
参考文献
Organic Letters, , vol. 15, # 4 p. 840 - 843
反应条件
zinc(II) chloride in 1,2-dichloro-ethane T=150°C; 0.25 h; microwave irradiation;
参考文献
Organic Letters, , vol. 8, # 22 p. 5065 - 5068
反应条件
1: 1.) NaNO2, H2SO4, 2.) KI, H2O / 1.) -10 deg C, 1 h, 2.) CHCl3, r.t., 2.5 h 2: 98 percent / Pd(PPh3)2Cl2, CuI / 20 h / Ambient temperature View Scheme
参考文献
Synlett, , # 6 p. 750 - 752
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Synthesis, , # 3 art. no. Z14204SS, p. 485 - 492
反应条件
(i) EtMgBr, THF, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1364 - 1366
