(4-溴苯基乙炔基)三甲基硅烷合成路线 （共 34 条）
反应条件
potassium carbonate
T=120 - 130°C; 0.25 h; microwave irradiation;
参考文献
Wettergren, Jenny; Minidis, Alexander B. E.
Tetrahedron Letters, 2003 , vol. 44, # 41 p. 7611 - 7612
反应条件
1: (4-bromophenylethynyl)trimethylsilane With n-butyllithium in tetrahydrofuran
T=-78°C;
2: dimethylmono-chlorosilane in tetrahydrofuran
参考文献
Wang, Fei; Kaafarani, Bilal R.; Neckers, Douglas C.
Macromolecules, 2003 , vol. 36, # 22 p. 8225 - 8230
反应条件
1: With n-butyllithium in diethyl ether
T=-78°C; 0.5 h;
2: With boric acid trimethyl ester in diethyl ether
T=-78 - 25°C; 14.5 h; Further stages.;
参考文献
Thoresen, Lars H.; Jiao, Guan-Sheng; Haaland, Wade C.; Metzker, Michael L.; Burgess, Kevin
Chemistry - A European Journal, 2003 , vol. 9, # 19 p. 4603 - 4610
反应条件
1: (4-bromophenylethynyl)trimethylsilane With n-butyllithium in diethyl ether
T=-78°C; Inert atmosphere;
2: dimethyl-dichlorosilane in diethyl ether
T=20°C; Inert atmosphere;
参考文献
Wang, Yike; Wang, Dengxu; Xu, Caihong; Wang, Rui; Han, Jianjun; Feng, Shengyu
Journal of Organometallic Chemistry, 2011 , vol. 696, # 18 p. 3000 - 3005
