反应条件
magnesium in diethyl ether stirring (over night, room temp.), rapidly addn. of germanium-complex, stirring (8 h), decantation (ice bath), quenching (NH4Cl); organic layer sepn., washing (water, sodium bicarbonate, water), drying (MgSO4), solvent removing (evapn.), chromy. work up (silica, hexane); elem. anal.;
参考文献
Toltl, Nicholas P.; Leigh, William J.
Journal of the American Chemical Society, 1998 , vol. 120, # 6 p. 1172 - 1178
