N-羟基-4-硝基苯甲酰胺合成路线 （共 20 条）
反应条件
phosphorus tribromide in benzene 5 h; Heating;
参考文献
Liguori, Angelo; Sindona, Giovanni; Romeo, Giovanni; Uccella, Nicola
Synthesis, 1987 , # 2 p. 168
反应条件
thionyl chloride; triethylamine 1.) benzene, reflux, 2.) ether; Multistep reaction;
参考文献
Zayed, Salem E.
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 108, # 1-4 p. 7 - 13
反应条件
ethanol; platinum Hydrogenation;
参考文献
Hackley et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 3651
反应条件
camphor-10-sulfonic acid in dichloromethane T=20°C; 25 h;
参考文献
Journal of Organic Chemistry, , vol. 67, # 14 p. 4833 - 4838
反应条件
1: With carbonyl diimidazole in acetonitrile T=20°C; Lossen rearrangement; 24 h; Inert atmosphere; 2: in acetonitrile T=60°C; Lossen rearrangement; Inert atmosphere;
参考文献
Vasantha, Basavalingappa; Hemantha, Hosahalli P.; Sureshbabu, Vommina V.
Synthesis, 2010 , # 17 art. no. P05010SS, p. 2990 - 2996
反应条件
1: p-nitrophenyl-N-hydroxycarbamate With 4-methyl-morpholine; bromo-dimethylsulfonium bromide in 1,2-dichloro-ethane
T=0°C; Lossen rearrangement; 2 h; Inert atmosphere;
2: morpholine in 1,2-dichloro-ethane
T=0 - 80°C; Lossen rearrangement;
参考文献
Yadav, Deepak K.; Yadav, Arvind K.; Srivastava, Vishnu P.; Watal, Geeta; Yadav, Lal Dhar S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2890 - 2893
反应条件
1: lead dioxide / ethyl acetate / 3 h / 0 °C
2: 70 mg / benzene / 12 h / Heating
View Scheme
参考文献
Mackay, Donald; Dao, Le H.; Dust, Julian M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2408 - 2416
参考文献
Mackay,D. et al.
Journal of the Chemical Society, Chemical Communications, 1977 , p. 702 - 703
反应条件
[bis(acetoxy)iodo]benzene in dichloromethane; N,N-dimethyl-formamide
T=0°C; Dehydrogenation; addition; 16 h;
参考文献
Adam, Waldemar; Bottke, Nils; Krebs, Oliver; Saha-Moeller, Chantu R.
European Journal of Organic Chemistry, 1999 , # 8 p. 1963 - 1965
反应条件
(i) NaH, benzene, (ii) /BRN= 2576714/, (iii) Et3N; Multistep reaction;
参考文献
Trani,A.; Bellasio,E.
Journal of Heterocyclic Chemistry, 1977 , vol. 14, p. 113 - 117
