反应条件
1: 91 percent / sodium hypophosphite / Raney Ni / pyridine; acetic acid; H2O / 2 h / 45 - 50 °C
2: 1) water, AcOH, 0 deg C, 2) RT, 3-4 h
3: 45 percent / propan-2-ol; H2O / Ambient temperature
View Scheme
参考文献
Oppolzer, W.; Grayson, J. I.; Wegmann, H.; Urrea, M.
Tetrahedron, 1983 , vol. 39, # 22 p. 3695 - 3706
