2-(4-硝基苯基)-1H-咪唑合成路线 (共 12 条)
反应条件
1: With tert-butyl methyl ether; nitric acid in tetrahydrofuran T=0°C; 2: With sulfuric acid in dichloromethane T=0°C; 1 h; Further stages.;
参考文献
Zhang, Pingsheng; Cedilote, Miall; Cleary, Thomas P.; Pierce, Michael E.
Tetrahedron Letters, 2007 , vol. 48, # 49 p. 8659 - 8664
反应条件
oxygen; carbon in xylene T=120°C; 25 h;
参考文献
Haneda, Satoshi; Okui, Ayaka; Ueba, Chigusa; Hayashi, Masahiko
Tetrahedron, 2007 , vol. 63, # 11 p. 2414 - 2417
反应条件
H6[PMo9V3O40] in acetonitrile T=90°C;
参考文献
Sadjadi, Samaheh; Heravi, Majid M.; Poormohammad, Nargess; Oskooie, Hossein A.; Beheshtiha, Yahya. Sh.; Bamoharram, Fatemeh F.
Synthetic Communications, 2009 , vol. 39, # 17 p. 3119 - 3125
反应条件
potassium hexacyano-ferrate in water T=20°C; 0.2 h;
参考文献
Shaikh, Kabeer A.; Patil, Vishal A.; Shaikh, Parveen A.
Chinese Journal of Chemistry, 2012 , vol. 30, # 4 p. 924 - 928
反应条件
1: 4-nitro-aniline With hydrogenchloride; sodium nitrite in water T=0 - 10°C; 2: 1H-imidazole With sodium acetate T=5 - 20°C;
参考文献
European Journal of Medicinal Chemistry, , vol. 44, # 6 p. 2347 - 2353
反应条件
1: para-nitro-benzonitrile With sodium methylate in methanol 2: 2-aminoacetaldehyde dimethyl acetal With acetic acid in methanol T=50°C; 3: With hydrogenchloride in methanol; water
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 5 p. 1573 - 1577
反应条件
1: 2-methyl-propan-2-ol / 20 °C 2: K2CO3; I2 / 2-methyl-propan-2-ol / 3 h / 70 °C 3: 73 percent / (diacetoxyiodo)benzene; K2CO3 / dimethylsulfoxide / 24 h / 20 °C View Scheme
参考文献
Synlett, , # 2 p. 227 - 230
反应条件
T=0 - 10°C; 5 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , p. 1489 - 1492
参考文献
Journal of the Chemical Society, , vol. 125, p. 2487
反应条件
beim Erhitzen ueber den Schmelzpunkt;
参考文献
Journal of the Chemical Society, , vol. 125, p. 2487