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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
161518-24-7
合成路线
（共 26 条）
1076-74-0
5-甲氧基-2-甲基吲哚
→
反应条件
161518-24-7
反应条件
1: trichlorophosphate / 0 - 20 °C 2: sodium hydride / N,N-dimethyl-formamide 3: nitric acid / acetic acid / 0 °C 4: tin; hydrogenchloride / ethanol / |Reflux 5: Fremy’s salt / acetone; aq. phosphate buffer / pH 6.4 6: sodium tetrahydroborate / methanol View Scheme
参考文献
Sharma, Kavita; Iyer, Aishwarya; Sengupta, Kundan; Chakrapani, Harinath
Organic Letters, 2013 , vol. 15, # 11 p. 2636 - 2639
6260-86-2
5-甲氧基-2-甲基-1H-吲哚-3-甲醛
→
反应条件
161518-24-7
反应条件
1: sodium hydride / N,N-dimethyl-formamide 2: nitric acid / acetic acid / 0 °C 3: tin; hydrogenchloride / ethanol / |Reflux 4: Fremy’s salt / acetone; aq. phosphate buffer / pH 6.4 5: sodium tetrahydroborate / methanol View Scheme
参考文献
Sharma, Kavita; Iyer, Aishwarya; Sengupta, Kundan; Chakrapani, Harinath
Organic Letters, 2013 , vol. 15, # 11 p. 2636 - 2639
34572-28-6
→
反应条件
161518-24-7
反应条件
1: nitric acid / acetic acid / 0 °C 2: tin; hydrogenchloride / ethanol / |Reflux 3: Fremy’s salt / acetone; aq. phosphate buffer / pH 6.4 4: sodium tetrahydroborate / methanol View Scheme
参考文献
Sharma, Kavita; Iyer, Aishwarya; Sengupta, Kundan; Chakrapani, Harinath
Organic Letters, 2013 , vol. 15, # 11 p. 2636 - 2639
161518-22-5
→
反应条件
161518-24-7
反应条件
1: 85 percent / potassium nitrodisulfonate / H2O; acetone / 2 h 2: 89 percent / NaBH4 / methanol / 2 h View Scheme
参考文献
Cotterill, Ann S.; Moody, Christopher J.; Mortimer, Roger J.; Norton, Claire L.; O'Sullivan, Noeleen; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 22 p. 3834 - 3843
13412-12-9
3-甲氧基氨基巴豆酸甲酯
→
反应条件
161518-24-7
反应条件
1.1: nitromethane / 24 h / 20 °C 2.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h 2.2: 3 h / 20 °C 3.1: acetic acid; nitric acid / 2 h / -10 - 20 °C 4.1: tin; hydrogenchloride / water; ethanol / 0.5 h / |Reflux 5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C View Scheme
参考文献
Schaefer, Anja; Burstein, Ethan S.; Olsson, Roger
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1944 - 1947
73975-59-4
→
反应条件
161518-24-7
反应条件
1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h 1.2: 3 h / 20 °C 2.1: acetic acid; nitric acid / 2 h / -10 - 20 °C 3.1: tin; hydrogenchloride / water; ethanol / 0.5 h / |Reflux 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C View Scheme
参考文献
Schaefer, Anja; Burstein, Ethan S.; Olsson, Roger
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1944 - 1947
480996-68-7
→
反应条件
161518-24-7
反应条件
1: acetic acid; nitric acid / 2 h / -10 - 20 °C 2: tin; hydrogenchloride / water; ethanol / 0.5 h / |Reflux 3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C View Scheme
参考文献
Schaefer, Anja; Burstein, Ethan S.; Olsson, Roger
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1944 - 1947
67-63-0
异丙醇
+
192820-78-3
→
反应条件
100-02-7
对硝基苯酚
+
161518-24-7
反应条件
Nitrous oxide in water γ-Irradiation; Kinetics;
参考文献
Swann; Moody; Stratford; Patel; Naylor; Vojnovic; Wardman; Everett
Journal of the Chemical Society, Perkin Transactions 2, 2001 , # 8 p. 1340 - 1345
67-63-0
异丙醇
→
反应条件
1849-36-1
4-硝基苯硫醇
+
161518-24-7
反应条件
Nitrous oxide in water γ-Irradiation; Kinetics;
参考文献
Swann; Moody; Stratford; Patel; Naylor; Vojnovic; Wardman; Everett
Journal of the Chemical Society, Perkin Transactions 2, 2001 , # 8 p. 1340 - 1345
67-63-0
异丙醇
→
反应条件
161518-24-7
反应条件
Nitrous oxide in water γ-Irradiation; Kinetics;
参考文献
Swann; Moody; Stratford; Patel; Naylor; Vojnovic; Wardman; Everett
Journal of the Chemical Society, Perkin Transactions 2, 2001 , # 8 p. 1340 - 1345
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