N-(1-甲基乙基)苯-1,4-二胺合成路线 (共 3 条)
反应条件
1-methyl-pyrrolidin-2-one in hydrogenchloride; water
参考文献
The Goodyear Tire and Rubber Company
Patent: US5019611 A1, 1991 ;
反应条件
hydrogenchloride; tin
T=90°C; 1 h;
参考文献
Parr, William J. E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3002 - 3007
反应条件
1: 1.) HCl, 2.) sodium cyanoborohydride / 1) methanol; 2) overnight
2: 69 percent / tin, aq. HCl / 1 h / 90 °C
View Scheme
参考文献
Parr, William J. E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3002 - 3007