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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
16155-95-6
合成路线
（共 11 条）
10531-80-3
6-甲基苯并恶唑
+
824-79-3
对甲苯亚磺酸钠
→
反应条件
16155-95-6
反应条件
palladium diacetate; copper (II) acetate monohydrate in 1,4-dioxane; diethylene glycol dimethyl ether T=120°C; 24 h; sealed vessel;
参考文献
Chen, Ru; Liu, Saiwen; Liu, Xinhua; Yang, Luo; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7675 - 7679
16308-16-0
4-碘化甲苯二乙酸酯
+
10531-80-3
6-甲基苯并恶唑
→
反应条件
16155-95-6
反应条件
1,10-phenanthroline; palladium diacetate; caesium carbonate in dimethyl sulfoxide T=150°C; 20 h; Inert atmosphere;
参考文献
Yu, Peng; Zhang, Guangyou; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4588 - 4590
10531-80-3
6-甲基苯并恶唑
+
1576-35-8
对甲苯磺酰肼
→
反应条件
16155-95-6
反应条件
dichloro bis(acetonitrile) palladium(II); 1,10-phenanthroline; tetrabutylammomium bromide; copper diacetate; sodium carbonate in 1,4-dioxane; dimethyl sulfoxide T=20 - 100°C; 4.58333 h; Inert atmosphere;
参考文献
Yu, Xinzhang; Li, Xingwei; Wan, Boshun
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 37 p. 7479 - 7482
104-87-0
对甲基苯甲醛
+
2835-98-5
6-氨基间甲酚
→
反应条件
16155-95-6
反应条件
copper ferrite; oxygen in toluene T=110°C; 24 h; Schlenk techniqueSealed tubeGreen chemistry;
参考文献
Yang, Daoshan; Zhu, Xiao; Wei, Wei; Sun, Nana; Yuan, Li; Jiang, Min; You, Jinmao; Wang, Hua
RSC Advances, 2014 , vol. 4, # 34 p. 17832 - 17839
25563-06-8
+
10531-80-3
6-甲基苯并恶唑
→
反应条件
16155-95-6
反应条件
dipotassium peroxodisulfate; 1,10-phenanthroline; palladium diacetate in dimethyl sulfoxide; toluene T=120°C; 24 h; air; chemoselective reaction;
参考文献
Li, Chengliang; Li, Pinhua; Yang, Jin; Wang, Lei
Chemical Communications, 2012 , vol. 48, # 35 p. 4214 - 4216
959031-87-9
→
反应条件
16155-95-6
反应条件
potassium carbonate; dimethyl sulfoxide T=140°C; Air atmosphere;
参考文献
Peng, Jinsong; Zong, Cuijuan; Ye, Min; Chen, Tonghui; Gao, Dewei; Wang, Yufeng; Chen, Chunxia
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 4 p. 1225 - 1230
2835-98-5
6-氨基间甲酚
+
104-85-8
对甲苯腈
→
反应条件
16155-95-6
反应条件
copper(II) bis(trifluoromethanesulfonate) in chlorobenzene 5 h; Reflux;
参考文献
Tan, Heng; Pan, Cheng-Xue; Xu, Yan-Li; Wang, Heng-Shan; Pan, Ying-Ming
Journal of Chemical Research, 2012 , vol. 36, # 6 p. 370 - 373
98-59-9
对甲苯磺酰氯
→
反应条件
16155-95-6
反应条件
1: hydrazine hydrate; water / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 2: dichloro bis(acetonitrile) palladium(II); sodium carbonate; copper diacetate; tetrabutylammomium bromide; 1,10-phenanthroline / dimethyl sulfoxide; 1,4-dioxane / 4.58 h / 20 - 100 °C / |Inert atmosphere View Scheme
参考文献
Yu, Xinzhang; Li, Xingwei; Wan, Boshun
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 37 p. 7479 - 7482
624-31-7
4-碘甲苯
→
反应条件
16155-95-6
反应条件
1: sodium periodate; sodium acetate; acetic acid / 2 h / Reflux 2: 1,10-phenanthroline; palladium diacetate; caesium carbonate / dimethyl sulfoxide / 20 h / 150 °C / Inert atmosphere View Scheme
参考文献
Yu, Peng; Zhang, Guangyou; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4588 - 4590
2835-98-5
6-氨基间甲酚
→
反应条件
16155-95-6
反应条件
1: 4 h / Reflux 2: 1,10-phenanthroline; palladium diacetate; caesium carbonate / dimethyl sulfoxide / 20 h / 150 °C / Inert atmosphere View Scheme
参考文献
Yu, Peng; Zhang, Guangyou; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4588 - 4590
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