甲烷磺酸 1-甲基丙基酯合成路线 （共 14 条）
反应条件
triethylamine in dichloromethane T=0 - 5°C; 1 h;
参考文献
Burns, Dennis H.; Miller, Jeffrey D.; Chan, Ho-Kit; Delaney, Michael O.
Journal of the American Chemical Society, 1997 , vol. 119, # 9 p. 2125 - 2133
反应条件
T=30°C; unter Druck;
参考文献
Proell; Adams
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 2217,2220
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Segall, Yoffi; Casida, John E.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 18, p. 209 - 212
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Segall, Yoffi; Casida, John E.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 18, p. 209 - 212
反应条件
T=30°C; unter Druck; analoge Reaktion mit anderen Alkansulfonsaeuren;
参考文献
Proell; Adams
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 2217,2220
反应条件
in tetrahydrofuran Mixt. was stirred at room temp. over night;; H2O and ether was added to a soln., layers were sepd.; organic layer was washed with 20percent KF and brine, then dried over K2CO3, mixt. was dissolved in hot EtOH, filtered, crystd. by cooling, ppt. was chromd. on silica column (pentane); elem. anal.;;
参考文献
Organometallics, , vol. 6, p. 415 - 420
参考文献
Zief; Fletcher; Kirshen
Journal of the American Chemical Society, 1946 , vol. 68, p. 2744
反应条件
tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide electroreduction;
参考文献
Shono, Tatsuya; Kashimura, Shigenori; Nogusa, Hideo
Chemistry Letters, 1986 , p. 425 - 428
反应条件
CuBr*Me2S-LiBr; lithium thiophenoxide; magnesium 1) THF, reflux, 2 h; 2) THF, HMPA, 67 deg C, 48 h; further reagents; Yield given. Multistep reaction;
参考文献
Burns, Dennis H.; Miller, Jeffrey D.; Chan, Ho-Kit; Delaney, Michael O.
Journal of the American Chemical Society, 1997 , vol. 119, # 9 p. 2125 - 2133
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=20°C; reduction at a platinum net at constant potential in the cathodic chamber;
参考文献
Sorensen, Heidi Skovbak; Daasbjerg, Kim
Acta Chemica Scandinavica, 1998 , vol. 52, # 1 p. 51 - 61
