甲烷磺酸 1-甲基丙基酯合成路线 (共 14 条)
反应条件
CuBr*Me2S-LiBr; lithium thiophenoxide; magnesium 1) THF, reflux, 2 h; 2) THF, HMPA, 67 deg C, 48 h; further reagents; Yield given. Multistep reaction;
参考文献
Burns, Dennis H.; Miller, Jeffrey D.; Chan, Ho-Kit; Delaney, Michael O.
Journal of the American Chemical Society, 1997 , vol. 119, # 9 p. 2125 - 2133
反应条件
trifluorormethanesulfonic acid T=80°C; 0.5 h;
参考文献
Kotsuki, Hiyoshizo; Ohishi, Takeshi; Inoue, Motoshi; Kojima, Tomoyuki
Synthesis, 1999 , # 4 p. 603 - 606
反应条件
trifluorormethanesulfonic acid T=80°C; 0.5 h;
参考文献
Kotsuki, Hiyoshizo; Ohishi, Takeshi; Inoue, Motoshi; Kojima, Tomoyuki
Synthesis, 1999 , # 4 p. 603 - 606
反应条件
tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide
electroreduction;
参考文献
Shono, Tatsuya; Kashimura, Shigenori; Nogusa, Hideo
Chemistry Letters, 1986 , p. 425 - 428