(S)-N-缩水甘油邻苯二甲酰亚胺合成路线 （共 18 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=0 - 20°C;
参考文献
WO2004/113301 A1, ;
Page 18 ;
WO 2004/113301 A1
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride in isopropyl alcohol T=10°C; 46 h;
参考文献
EP1403267 A1, ;
Page 5 ;
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride in isopropyl alcohol T=40°C; 22 h;
参考文献
EP1403267 A1, ;
Page 6-7 ;
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; 4 h;
参考文献
WO2007/30761 A2, ;
Page/Page column 37; 98-99 ;
WO 2007/030761 A2
反应条件
potassium carbonate in methanol T=0°C; 1 h;
参考文献
WO2006/31179 A1, ;
Page/Page column 5 ;
反应条件
1: With N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate in isopropyl alcohol T=20 - 40°C; 2: With potassium tert-butylate in isopropyl alcohol T=5 - 10°C;
参考文献
WO2012/41263 A2, ;
Page/Page column 9-10 ;
反应条件
tetrabutylammomium bromide; potassium carbonate in acetone T=35 - 60°C; 12 h;
参考文献
WO2013/98833 A2, ;
Page/Page column 41 ;
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride in DMF (N,N-dimethyl-formamide) T=20°C; 16 h;
参考文献
EP1403267 A1, ;
Page 6 ;
反应条件
potassium phosphate in 1,2-dichloro-ethane T=80°C; 14 h; Product distribution / selectivity;
参考文献
WO2007/132990 A1, ;
Page/Page column 8-10 ;
反应条件
in tetrahydrofuran; water
