3-甲基丁-3-烯酸乙酯合成路线 (共 22 条)
反应条件
piperidine in tetrahydrofuran
参考文献
Miginiac,P.; Zamlouty,G.
Journal of Organometallic Chemistry, 1975 , vol. 96, p. 163 - 168
反应条件
1: (i) aq. NaOH, EtOH, (ii) /BRN= 102415/ 2: (i) BF3-Et2O, (ii) aq. HCl View Scheme
参考文献
Smith,A.B. et al.
Tetrahedron Letters, 1975 , p. 4225 - 4228
反应条件
methanesulfonic acid
T=70°C; 2 h;
参考文献
Lakner, Frederick J.; Hager, Lowell P.
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3923 - 3925
反应条件
palladium diacetate; triphenylphosphine
T=50°C; P=7600 Torr; 8 h;
参考文献
Tsuji, Jiro; Sato, Koji; Okumoto, Hiroshi
Tetrahedron Letters, 1982 , vol. 23, # 49 p. 5189 - 5190
反应条件
in acetone; tert-butyl alcohol
Irradiation;
参考文献
Itoh,M. et al.
Tetrahedron, 1968 , vol. 24, p. 6591 - 6600
反应条件
Ni(PPh3)4 in N,N,N',N',N'',N''-hexamethylphosphoric triamide
3 h; Heating;
参考文献
Fauvarque, J.F.; Jutand, A.
Journal of Organometallic Chemistry, 1981 , vol. 209, # 1 p. 109 - 114
参考文献
McElvain; Morris
Journal of the American Chemical Society, 1952 , vol. 74, p. 2657,2661
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
反应条件
1: potassium tert-butylate; tert-butyl alcohol / 110 °C
2: potassium tert-butylate / 100 °C
3: diluted aqueous acetic acid
View Scheme
参考文献
McElvain; Morris
Journal of the American Chemical Society, 1952 , vol. 74, p. 2657,2661
反应条件
1: potassium tert-butylate / 100 °C
2: diluted aqueous acetic acid
View Scheme
参考文献
McElvain; Morris
Journal of the American Chemical Society, 1952 , vol. 74, p. 2657,2661