3-甲基丁-3-烯酸乙酯合成路线 （共 22 条）
反应条件
1: aqueous sulfuric acid / Beim Behandeln anschliessend mit Eis
2: pyridine
View Scheme
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
反应条件
palladium diacetate; potassium carbonate
T=20°C; P=760 Torr; 0.833333 h;
参考文献
Kiji, Jitsuo; Okano, Tamon; Higashimae, Yukiko; Fukui, Yasuyuki
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 4 p. 1029 - 1031
反应条件
1: m-chloroperbenzoic acid / CH2Cl2
2: CCl4
View Scheme
参考文献
Aue,D.H.; Thomas,D.
Journal of Organic Chemistry, 1974 , vol. 39, p. 3855 - 3862
反应条件
triethylamine; phosphonic acid diethyl ester
T=80°C; 30 h; Yield given. Yields of byproduct given;
参考文献
Hirao, Toshikazu; Fujihara, Yoshimi; Kurokawa, Ken; Ohshiro, Yoshiki; Agawa, Toshio
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2830 - 2832
反应条件
zinc salt
und Zersetzen des β-Methyl-β-carbaethoxy-methyl-propiolactons durch Destillation;
参考文献
Eastman Kodak Co.
Patent: US2450131 , 1946 ;
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Eastman Kodak Co.
Patent: US2450118 , 1947 ;
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Eastman Kodak Co.
Patent: US2450116 , 1947 ;
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Eastman Kodak Co.
Patent: US2450117 , 1947 ;
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Hagemeyer
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 769
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Eastman Kodak Co.
Patent: US2450133 , 1946 ;
反应条件
in tetrachloromethane
参考文献
Aue,D.H.; Thomas,D.
Journal of Organic Chemistry, 1974 , vol. 39, p. 3855 - 3862
反应条件
T=111°C; Decarboxylation; Rate constant;
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
反应条件
T=111°C; Decarboxylation; Rate constant;
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
反应条件
T=111°C; Decarboxylation; Rate constant;
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
反应条件
(i) Zn, HgI2, (ii) (hydrolysis); Multistep reaction;
参考文献
Couffignal,R.; Gaudemar,M.
Journal of Organometallic Chemistry, 1975 , vol. 96, p. 149 - 162
