(9ci)-6-乙烯-3-吡啶甲腈合成路线 (共 2 条)
反应条件
triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in methanol T=20 - 80°C; 8 h; Sealed tube; Product distribution / selectivity;
参考文献
SCHERING CORPORATION
Patent: WO2009/5646 A2, 2009 ;
Location in patent: Page/Page column 158 ;
WO 2009/005646 A2
反应条件
1: With ozone in dichloromethane T=-78°C; 0.5 h; 2: With dimethylsulfide in dichloromethane T=-78 - 20°C; 18 h;
参考文献
SCHERING CORPORATION
Patent: WO2009/5646 A2, 2009 ;
Location in patent: Page/Page column 147 ;
WO 2009/005646 A2